Liquid extraction


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Liquid-Liquid Extraction Applications by Industry

Cooney, D. Solvent extraction of phenol from aqueous solution in a hollow fiber device. Dahuron, L. Protein extractions with hollow fibers.

Perspectives on the Use of Liquid Extraction for Radioisotope Purification

Dahuron, and E. Liquid-liquid extractions with microporous hollow fibers. De Haan, A.

Requirements for the solvent

Bartels, and J. Extraction of metal ions from waste water.

Liquid-Liquid extraction

Modelling of the mass transfer in a supportedliquid-membrane process. Dekker, M. Wijnans, J. Baltussen, B. Bijsterbosch, and C. Fournier, R. Mathematical model of microporous hollow-fiber membrane extractive fermentor. Frank, G. Membrane solvent extraction with hydrophobic microporous hollow fiber and extractive bioreactor development for fuel ethanol production.

Alcohol production by yeast fermentation and membrane extraction. An integrated bioreactor-separator: In-situ recovery of fermentation products by a novel dispersion-free solvent extraction technique. Hanson, C. Lo, and M. Solvent Extraction Handbook. Ho, W. Lee, and K. Membrane hydrometallurgical extraction process. Patent 3,— Hoq, M. Yamane, and S. Continuous hydrolysis of olive oil by lipase in a microporous hydrophobic membrane bioreactor. JAOCS 62 6 — Kang, W.

Hollow fiber membrane-based extractive bioreactors and a whole cell immobilization technique. Shukla, G. Frank, and K. Evaluation of O 2 and CO 2 transfer coefficients in a locally integrated tubular hollow fiber bioreactor. Shukla, and K. Ethanol production in a microporous hollow-fiber based extractive fermentor with immobilized yeast. Keller, K. A two-dimensional analysis of porous membrane transport. Khare, S. Nondispersive membrane solvent extraction using asymmetric ceramic membranes. Kiani, A. Bhave, and K.

Liquid/Liquid Extraction

Solvent extraction with immobilized interfaces in a microporous hydrophobic membrane. Kim, B. Membrane-based extraction for selective removal and recovery of metals. Critical entry pressure for liquids in hydrophobic membranes. Colloid Interface Sci. Lee, L. Ho, and K. Membrane solvent extraction. Patent 3,, Malone, D. Diffusional boundary-layer resistance for membranes with low porosity. Matsumoto, M.

Shimauchi, K. Kondo, and F. Kinetics of copper extraction with Kelex using a hollow fiber membrane extractor. Solvent Extr. Ion Exch. Misek, T. Rugby, U. Naser, S. A numerical evaluation of a hollow fiber extractive fermentor process for the production of ethanol. Newman, J. Extension of Leveque solution. Series C J. Heat Trans. Park, J. Flow distribution in the lumen side of a hollow-fiber module. Prasad, R. Bhave, A. Kiani, and K. Further studies on solvent extraction with immobilized interfaces in a microporous hydrophobic membrane.

Nondispersive solvent extraction using micro-porous membranes.

Liquid-Liquid Extraction

AIChE Symp. Khare, A. Sengupta, and K.

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To remove a phase from the separatory funnel, return the funnel to its upright position and rest it on a ring clamp. Remove the cap from the separatory funnel and drain the two phases into two different beakers. Decide which solvent contains the target compound and place the appropriate beaker in a 'safe place' probably in a corner of the bench, but always in the hood. Usually the entire extraction process is repeated several times to insure that the maximum amount of the target molecule has been isolated. For this reason it is necessary to also save the phase containing the original mixture.

Common Source of Error The most common source of confusion for students often occurs when deciding which solvent in the separatory funnel contains the target molecule. This requires some knowledge of the polarity of the target molecule and the extraction solvents used. If ether and water are the extraction solvents and the target molecule is nonpolar, then the ether layer would contain most of the target compound 'like dissolves like' after the first extraction. If this were a real extraction , the bottom layer aqueous would be drained and stored in a separate beaker from the ether. After draining the ether, the aqueous phase would be returned to the separatory funnel and the entire process repeated to insure maximum recovery of the target compound.

The ether layers would then be combined and extraction complete. Multiple extractions with small amounts of volume are always more efficient than one single extraction with large volume. This is a direct result of the distribution coefficient and will be discussed in class. I opened the stopcock to drain the layers and nothing happened. Occasionally a contaminate may become lodged in the stopcock. For this reason it is always good practice to wash the separatory funnel before attempting extraction and checking to be sure it drains properly.

The common problem, however, is that the cap has been mistakenly left on the separatory funnel while attempting to drain. This establishes a vacuum within the separatory funnel and will not allow any liquid to drain. Sometimes an 'apparent' third layer appears between the top and bottom layers. This third layer is actually an interface between the two layers and generally appears only as the layers are separating. Leaving the separatory funnel undisturbed for a few minutes until the layers have completely separated usually eliminates the problem.

Alternatively, gently rocking the separatory funnel is another viable solution.


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If neither of these suggestions work, check with your TA - there are many other reasons why three layers have appeared. Remember when performing successive extractions to 'keep your eye on the prize. Return the aqueous layer to the separatory funnel for a second extraction. This will remove most of the target molecule from the aqueous phase. It does absolutely no good to extract ether with ether. If you are using ether and water as the extraction solvents, ether is always the top layer because it is less dense than water.

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Liquid extraction Liquid extraction
Liquid extraction Liquid extraction
Liquid extraction Liquid extraction
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